(S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester

Base Information

• Chemical Name: (S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester
• CAS No.: 131550-37-3
• Molecular Formula: C₂₁H₂₇NO₇
• Molecular Weight: 405.448

Synonyms:(S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester

Chemical Property of (S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester

Chemical Property:

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Technology Process of (S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester

There total 1 articles about (S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester (30925-18-9) + magnesium monoallyl malonate (126690-67-3) → (S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester (131550-37-3)

Guidance literature:

With 1,1'-carbonyldiimidazole; In acetonitrile; at 25 ℃;

DOI:10.1016/S0040-4039(00)97050-3

Reference yield: 68.0%

(S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester (131550-37-3) + methyl iodide (74-88-4) → (S)-5-tert-Butoxycarbonylamino-2,2-dimethyl-3-oxo-hexanedioic acid 1-allyl ester 6-benzyl ester (131550-39-5)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

DOI:10.1016/S0040-4039(00)97050-3

Reference yield: 58.0%

(S)-2-tert-Butoxycarbonylamino-4-oxo-hexanedioic acid 6-allyl ester 1-benzyl ester (131550-37-3) + methyl iodide (74-88-4) → (S)-5-tert-Butoxycarbonylamino-2-methyl-3-oxo-hexanedioic acid 1-allyl ester 6-benzyl ester (131550-38-4)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

DOI:10.1016/S0040-4039(00)97050-3

upstream raw materials:

2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester

magnesium monoallyl malonate

Downstream raw materials:

1-((S)-3-Benzyloxycarbonyl-3-tert-butoxycarbonylamino-propionyl)-cyclopentanecarboxylic acid allyl ester

(S)-5-tert-Butoxycarbonylamino-2-butyl-3-oxo-hexanedioic acid 1-allyl ester 6-benzyl ester

(S)-5-tert-Butoxycarbonylamino-2-hexyl-3-oxo-hexanedioic acid 1-allyl ester 6-benzyl ester

(S)-2-Benzyl-5-tert-butoxycarbonylamino-3-oxo-hexanedioic acid 1-allyl ester 6-benzyl ester

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