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C17H25N5O3

Base Information Edit
C<sub>17</sub>H<sub>25</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C17H25N5O3

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Chemical Property of C17H25N5O3 Edit
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Technology Process of C17H25N5O3

There total 4 articles about C17H25N5O3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Boc-Leu-NHiPr; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;
C8H7N3O3; With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo300063u
Guidance literature:
Multi-step reaction with 4 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.08 h / -5 - -3 °C / Inert atmosphere
1.2: Inert atmosphere
1.3: 2 h / 0 °C / Inert atmosphere
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 12 h / 20 °C / Inert atmosphere
3.2: pH 4
4.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
4.2: 12 h / 20 °C / Inert atmosphere
With hydrogenchloride; lithium hydroxide monohydrate; potassium carbonate; trifluoroacetic acid; potassium iodide; sodium nitrite; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo300063u
Guidance literature:
Multi-step reaction with 2 steps
1.1: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
2.2: 12 h / 20 °C / Inert atmosphere
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo300063u
upstream raw materials:

C8H7N3O3

N-tert-butoxycarbonyl-L-leucine

2-azidophenol

2-amino-phenol

Downstream raw materials:

C33H45N7O6

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