2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

Base Information

Chemical Name:2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate
CAS No.:1178586-92-9
Molecular Formula:C₁₅H₁₁FNO₆P
Molecular Weight:351.228
Hs Code.:

Synonyms:2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

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Chemical Property of 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

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Technology Process of 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

There total 2 articles about 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1178586-90-7
diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

: 1178586-92-9
2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

Guidance literature:: diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate; With trimethylsilyl bromide; In dichloromethane; for 23h; Reflux;

With methanol; for 0.333333h;

Reference yield:

: 524684-52-4
prinaberel

: 1178586-92-9
2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 17 h / 20 °C

2.1: trimethylsilyl bromide / dichloromethane / 23 h / Reflux

2.2: 0.33 h

With trimethylsilyl bromide; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;