diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

Base Information

Chemical Name:diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate
CAS No.:1178586-90-7
Molecular Formula:C₁₉H₁₉FNO₆P
Molecular Weight:407.335
Hs Code.:

Synonyms:diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

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Chemical Property of diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

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Technology Process of diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

There total 2 articles about diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 598-02-7
Diethyl phosphate

: 524684-52-4
prinaberel

: 1178586-90-7
diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; tetrachloromethane; acetonitrile; at 20 ℃; for 24h;

Reference yield: 62.0%

: 814-49-3
diethyl chlorophosphate

: 524684-52-4
prinaberel

: 1178586-90-7
diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 17h;

Reference yield: 94.0%

: 1178586-90-7
diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate

: 1178586-92-9
2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl dihydrogen phosphate

Guidance literature:: diethyl 2-fluoro-4-(5-hydroxy-7-vinylbenzo[d]oxazol-2-yl)phenyl phosphate; With trimethylsilyl bromide; In dichloromethane; for 23h; Reflux;

With methanol; for 0.333333h;