3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

Base Information

Chemical Name:3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline
CAS No.:528584-25-0
Molecular Formula:C₁₇H₁₂Cl₂N₄OS
Molecular Weight:391.28
Hs Code.:

Synonyms:3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

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Chemical Property of 3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

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Technology Process of 3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

There total 3 articles about 3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 79-04-9
chloroacetyl chloride

: 74323-84-5
2-amino-4-(2-chlorophenyl)-5-phenylazothiazole

: 528584-25-0
3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

Guidance literature:: With triethylamine; In benzene; at 20 ℃; for 2h;
DOI:10.1002/jhet.5570390604

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 528584-25-0
3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / iodine / 12 h / Heating

2: 90 percent / aq. sodium nitrite; HCl; sodium acetate / aq. ethanol / 2 h / -5 °C

3: 85 percent / triethylamine / benzene / 2 h / 20 °C

With hydrogenchloride; iodine; sodium acetate; triethylamine; sodium nitrite; In ethanol; benzene;
DOI:10.1002/jhet.5570390604

Reference yield:

: 21344-90-1
4-(o-chlorophenyl)-1,3-thiazol-2-amine

: 528584-25-0
3-chloromethylcarbonyl-4-(2-chlorophenyl)-2-imino-5-phenylazo-thiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / aq. sodium nitrite; HCl; sodium acetate / aq. ethanol / 2 h / -5 °C

2: 85 percent / triethylamine / benzene / 2 h / 20 °C

With hydrogenchloride; sodium acetate; triethylamine; sodium nitrite; In ethanol; benzene;
DOI:10.1002/jhet.5570390604