1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose
CAS No.:1053703-50-6
Molecular Formula:C₄₁H₃₄N₄O₁₃
Molecular Weight:790.74
Hs Code.:

Synonyms:1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

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Chemical Property of 1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

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Technology Process of 1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

There total 1 articles about 1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 67546-20-7
1,6-anhydro-2-azido-2-deoxy-β-D-glucopyranose

: 3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-D-glucopyranosyl 2,2,2-trichloroacetimidate

: 1,6-anhydro-2-azido-3,4-di-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

: 1053703-50-6
1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

Guidance literature:: With molecular sieve; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; Ambient temperature;
DOI:10.1021/jo980735a

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 1053703-50-6
1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

: 214117-49-4
1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

Guidance literature:: With pyridine; dmap; In dichloromethane; for 72h; Ambient temperature;
DOI:10.1021/jo980735a

Reference yield:

: 1053703-50-6
1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

: C₄₈H₄₀N₂O₁₄

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine, DMAP / CH₂Cl₂ / 72 h / Ambient temperature

2: H₂ / Pd/C / methanol / 4 h / Ambient temperature

With pyridine; dmap; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jo980735a