1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose
CAS No.:214117-49-4
Molecular Formula:C₄₈H₃₈N₄O₁₄
Molecular Weight:894.848
Hs Code.:

Synonyms:1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

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Chemical Property of 1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

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Technology Process of 1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

There total 1 articles about 1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 1053703-50-6
1,6-anhydro-2-azido-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

: 214117-49-4
1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

Guidance literature:: With pyridine; dmap; In dichloromethane; for 72h; Ambient temperature;
DOI:10.1021/jo980735a

Reference yield:

: 214117-49-4
1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

: C₄₈H₄₀N₂O₁₄

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4h; Ambient temperature;
DOI:10.1021/jo980735a

Reference yield:

: 214117-49-4
1,6-anhydro-2-azido-3-O-benzoyl-4-O-(3,4,6-tri-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranose

: 214117-41-6
C₅₁H₄₁Cl₃N₂O₁₆

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 4 h / Ambient temperature

2: NEt₃ / CH₂Cl₂ / Ambient temperature

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jo980735a