ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

Base Information

Chemical Name:ethyl DL-phenylglycinate hydrogen p-toluenesulfonate
CAS No.:36123-72-5
Molecular Formula:C₇H₈O₃S*C₁₀H₁₃NO₂
Molecular Weight:351.423
Hs Code.:

Synonyms:ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

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Chemical Property of ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

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Technology Process of ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

There total 1 articles about ethyl DL-phenylglycinate hydrogen p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 64-17-5
ethanol

: 104-15-4
toluene-4-sulfonic acid

: 2835-06-5
phenylglycin

: 36123-72-5
ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

Guidance literature:: In benzene; for 48h; Heating;

Reference yield: 75.0%

: 100-52-7
benzaldehyde

: 36123-72-5
ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

: 77290-52-9
N-benzyliden-2-phenylglycine ethyl ester

Guidance literature:: With magnesium sulfate; triethylamine; In dichloromethane; for 4h; Ambient temperature;

Reference yield: 43.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 36123-72-5
ethyl DL-phenylglycinate hydrogen p-toluenesulfonate

: 749874-56-4
N-[(phenyl)(pyrrolidin-1-yl)methylene]benzamide

: 484-47-9
lophine

Guidance literature:: trifluoromethylsulfonic anhydride; N-[(phenyl)(pyrrolidin-1-yl)methylene]benzamide; In dichloromethane; at -50 ℃; for 1.5h;

ethyl DL-phenylglycinate hydrogen p-toluenesulfonate; With triethylamine; In dichloromethane; at 20 ℃; for 16h; Further stages.;
DOI:10.1002/ejoc.200400057