(1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

Base Information

Chemical Name:(1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate
CAS No.:213909-04-7
Molecular Formula:C₂₉H₂₄O₄
Molecular Weight:436.507
Hs Code.:

Synonyms:(1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

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Chemical Property of (1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

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Technology Process of (1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

There total 4 articles about (1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 213909-03-6
(1R,2R)-1,2-diphenyl-2-benzyloxyethanol

: 611-73-4
Benzoylformic acid

: 213909-04-7
(1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4020(98)00657-7

Reference yield:

: 52340-78-0
(R,R)-hydroxybenzoin

: 213909-04-7
(1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 92 percent / DIBAL / toluene / 2 h / 0 °C

3: 91 percent / N,N-dimethylaminopyridine; DCC / CH₂Cl₂ / 0 °C

With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; toluene-4-sulfonic acid; In dichloromethane; toluene; benzene; 1: Cycloaddition / 2: Reduction / 3: Esterification;
DOI:10.1016/S0040-4020(98)00657-7

Reference yield:

: 100-52-7
benzaldehyde

: 213909-04-7
(1R,2R)-1,2-diphenyl-2-benzyloxyethyl phenylglyoxalate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 92 percent / DIBAL / toluene / 2 h / 0 °C

3: 91 percent / N,N-dimethylaminopyridine; DCC / CH₂Cl₂ / 0 °C

With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; toluene-4-sulfonic acid; In dichloromethane; toluene; benzene; 1: Cycloaddition / 2: Reduction / 3: Esterification;
DOI:10.1016/S0040-4020(98)00657-7