N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine

Base Information

• Chemical Name: N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine
• CAS No.: 1353585-07-5
• Molecular Formula: C₁₉H₁₅B₂NO₄
• Molecular Weight: 342.954
• Mol file: 1353585-07-5.mol

Synonyms:N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine

Chemical Property of N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine

There total 3 articles about N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzonitrile (100-47-0) + benzo[1,3,2]dioxaborole (274-07-7) → N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine (1353585-07-5)

Guidance literature:

[Mo(H)(Cl)(P(CH₃)3)3(N(C₆H₃(CH₃CHCH₃)2))]; In benzene-d6; react. of HBCat with 0.4 M soln. of PhCN (2:1 molar ratio) in C6D6 at temp. of 22°C for 12 h in presence of 5 mol% of Mo complex as catalyst; detd. by NMR;

DOI:10.1039/c1cc14508h

Reference yield:

(2,6-diisopropyl-C6H3-N)Mo(IV)(H)(Cl){η2-(CatB)NCHPh}(PMe3)2 + benzonitrile (100-47-0) + benzo[1,3,2]dioxaborole (274-07-7) → N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine (1353585-07-5) + C25H41ClMoN2P2

Guidance literature:

In benzene-d6; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1039/c5dt02945g

Reference yield:

benzophenone (119-61-9) + benzonitrile (100-47-0) + benzo[1,3,2]dioxaborole (274-07-7) → Ph2CH(OBCat) (1353585-10-0) + N-(benzo[d][1,3,2]dioxaborol-2-yl)-N-benzylbenzo[d][1,3,2]dioxaborol-2-amine (1353585-07-5)

Guidance literature:

With tetramethylsilane; (2,6-diisopropylphenyl-N=)Mo(H)(Cl)(PMe₃)3; In benzene-d6; at 22 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c1cc14508h

upstream raw materials:

benzophenone

benzonitrile

benzo[1,3,2]dioxaborole

Downstream raw materials:

bis(benzo-1,3,2-dioxoborolanyl)oxide

N-benzylidene benzylamine