4-[2-(2,5-Dimethoxyphenyl)vinyl]aniline

Base Information

Chemical Name:4-[2-(2,5-Dimethoxyphenyl)vinyl]aniline
CAS No.:23435-31-6
Molecular Formula:C16H17 N O2
Molecular Weight:255.34
Hs Code.:2922199090
European Community (EC) Number:250-942-3
DSSTox Substance ID:DTXSID6020482
Nikkaji Number:J150.040F,J154.142K
ChEMBL ID:CHEMBL1173699
Mol file:23435-31-6.mol

Synonyms:4-[2-(2,5-dimethoxyphenyl)vinyl]aniline;23435-31-6;4-[(E)-2-(2,5-Dimethoxyphenyl)ethenyl]aniline;BRN 2855929;4-(2,5-Dimethoxy)stilbenamine;4'-Stilbenamine, 2,5-dimethoxy-;4-(2,5-Dimethoxyphenethyl)aniline;2,5-Dimethoxy-4'-aminostilbene(trans);4'-AMINO-2,5-DIMETHOXY STILBENE;CHEMBL1173699;4-(2-(2,5-Dimethoxyphenyl)ethyl)benzenamine;2,5-Dimethoxy-4'-aminostilbene;2',5'-Dimethoxy-4-stilbenamine;Stilbenamine, 2',5'-dimethoxy-;4-(2-(2,5-Dimethoxyphenyl)vinyl)aniline;Benzenamine, 4-(2-(2,5-dimethoxyphenyl)ethyl)-;5803-51-0;Benzenamine, 4-(2-(2,5-dimethoxyphenyl)ethenyl)-;Benzenamine, 4-[2-(2,5-dimethoxyphenyl)ethenyl]-;D0W7GU;SCHEMBL4580454;DTXSID6020482;OZGXSMOLBWHIQA-ZZXKWVIFSA-N;BDBM50322049;(E)-4-(2,5-dimethoxystyryl)aniline;(E)-2',5'-Dimethoxy-4-stilbenamine;2,5-Dimethoxy-4'-amino-trans-stilbene;2,5-Dimethoxy-4''-amino-trans-stilbene;PD180174;LS-146770;4-[(E)-2-(2,5-Dimethoxyphenyl)ethenyl]aniline #;Q63088188;Benzenamine, 4-(2-(2,5-dimethoxyphenyl)ethyl)- (9CI);Benzenamine, 4-[2-(2,5-dimethoxyphenyl)ethenyl]-, (E)-

Suppliers and Price of 4-[2-(2,5-Dimethoxyphenyl)vinyl]aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-[2-(2,5-Dimethoxyphenyl)vinyl]aniline

Chemical Property:

Vapor Pressure:9.21E-08mmHg at 25°C
Melting Point:91-92 °C
Refractive Index:1.5500 (estimate)
Boiling Point:441.6°Cat760mmHg
PKA:4.31±0.10(Predicted)
Flash Point:244.3°C
PSA：44.48000
Density:1.145g/cm³
LogP:4.03760
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:255.125928785
Heavy Atom Count:19
Complexity:285

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)OC)C=CC2=CC=C(C=C2)N
Isomeric SMILES:COC1=CC(=C(C=C1)OC)/C=C/C2=CC=C(C=C2)N

Technology Process of 4-[2-(2,5-Dimethoxyphenyl)vinyl]aniline

There total 2 articles about 4-[2-(2,5-Dimethoxyphenyl)vinyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 14568-68-4
1,4-dimethoxy-2-vinylbenzene

: 540-37-4
p-aminoiodobenzene

: 23435-31-6,32180-65-7
2,5-dimethoxy-4'-amino-trans-stilbene

Guidance literature:: With tetrabutylammomium bromide; potassium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 20 - 80 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.05.042

Reference yield:

: 23435-31-6,32180-65-7
2,5-dimethoxy-4'-amino-trans-stilbene

Guidance literature:: entspr. Nitroverb., Ra-Ni;
DOI:10.1021/jo00829a057

Reference yield: 75.0%

: (tris(3,5-dimethylpyrazol-1-yl)hydroborate)(nitrosyl)diiodomolybdenum-toluene (1/1)

: 23435-31-6,32180-65-7
NH₂C₆H₄CHCHC₆H₃(OCH₃)2

: [Mo(NO)(HB(3,5-dimethylpyrazolyl)3)I(NHC₆H₄CH=CHC₆H₃(OMe)2-2,5)]

Guidance literature:: With NEt₃; In toluene; N2-atmosphere; refluxing of stoich. amts. (3 h); evapn. to dryness (reduced pressure), chromy. (SiO2, CH2Cl2), crystn.; elem. anal.;
DOI:10.1039/DT9950000673