1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

Base Information

Chemical Name:1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone
CAS No.:1176981-06-8
Molecular Formula:C₁₈H₁₉N₃O₄
Molecular Weight:341.367
Hs Code.:

Synonyms:1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

Suppliers and Price of 1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

There total 2 articles about 1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 189333-46-8
9-benzyl-2,4-dioxo-3,9-diazaspiro[5,5]undecane-1,5-dicarbonitrile

: 1176981-06-8
1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

Guidance literature:: With sulfuric acid; In water; at 60 - 90 ℃; for 2h; Large scale;

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 1176981-06-8
1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium acetate; ammonium hydroxide / methanol / 21 h / 0 - 20 °C

2.1: sulfuric acid / 4 h / 60 °C

2.2: 1 h / 100 °C

With ammonium hydroxide; sulfuric acid; ammonium acetate; In methanol;

Reference yield: 98.5%

: 1176981-06-8
1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone

: 189333-49-1
3-benzyl-3,9-diazaspiro[5.5]undecane

Guidance literature:: 1'-benzyl-3,7-diazaspiro[bicyclo[3.3.1]nonane-9,4'-piperidine]-2,4,6,8-tetraone; With sodium bis(2-methoxyethoxy)aluminium dihydride; In xylene; at 0 - 127 ℃;

With water; sodium hydroxide; In xylene; at 0 ℃; for 0.583333h;