3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

Base Information

Chemical Name:3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone
CAS No.:1355037-43-2
Molecular Formula:C₇₄H₁₃₁ClN₂OS₆
Molecular Weight:1292.72
Hs Code.:

Synonyms:3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

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Chemical Property of 3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

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Technology Process of 3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

There total 6 articles about 3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 1355037-47-6
3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

: 1355037-43-2
3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja209467h

Reference yield:

: 1355037-27-2
3,4,5-tridecylsulfanylbenzaldehyde

: 1355037-34-1
(3,4,5-tri(decylsulfanyl)phenyl)hydrazine

: 1355037-43-2
3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 0.5 h / Reflux; Inert atmosphere

2: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

With pyridine; acetic acid; In ethanol; dichloromethane;
DOI:10.1021/ja209467h

Reference yield:

: 138526-69-9
3,4,5-trifluoro-1-bromobenzene

: 1355037-43-2
3,4,5-tridecylsulfanylbenzaldehyde α-chloroformyl-3',4',5'-tridecylsulfanylphenylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1.1: 60 - 80 °C

2.1: n-butyllithium / tetrahydrofuran

2.2: -78 °C

3.1: acetic acid / ethanol / Reflux

4.1: pyridine / dichloromethane / 20 °C

With pyridine; n-butyllithium; acetic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1080/10426507.2012.736896