3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

Base Information

Chemical Name:3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone
CAS No.:1355037-47-6
Molecular Formula:C₇₃H₁₃₂N₂S₆
Molecular Weight:1230.26
Hs Code.:

Synonyms:3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

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Chemical Property of 3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

Chemical Property:

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Technology Process of 3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

There total 5 articles about 3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355037-27-2
3,4,5-tridecylsulfanylbenzaldehyde

: 1355037-34-1
(3,4,5-tri(decylsulfanyl)phenyl)hydrazine

: 1355037-47-6
3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

Guidance literature:: With acetic acid; In ethanol; for 0.5h; Reflux; Inert atmosphere;
DOI:10.1021/ja209467h

Reference yield:

: 138526-69-9
3,4,5-trifluoro-1-bromobenzene

: 1355037-47-6
3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 60 - 80 °C

2.1: n-butyllithium / tetrahydrofuran

2.2: -78 °C

3.1: acetic acid / ethanol / Reflux

With n-butyllithium; acetic acid; In tetrahydrofuran; ethanol;
DOI:10.1080/10426507.2012.736896

Reference yield:

: 40520-16-9
sodium n-decylthiolate

: 1355037-47-6
3,4,5-trioctylsulfanylbenzaldehyde 3,4,5-trioctylsulfanylphenylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 60 - 80 °C

2.1: n-butyllithium / tetrahydrofuran

2.2: -78 °C

3.1: acetic acid / ethanol / Reflux

With n-butyllithium; acetic acid; In tetrahydrofuran; ethanol;
DOI:10.1080/10426507.2012.736896