ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

Base Information

Chemical Name:ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate
CAS No.:1316844-45-7
Molecular Formula:C₁₇H₁₉NO₄
Molecular Weight:301.342
Hs Code.:

Synonyms:ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

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Chemical Property of ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

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Technology Process of ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

There total 5 articles about ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1316844-32-2
C₂H₃O₂^(1-)*C₂₁H₂₁INO₂⁽¹⁺⁾

: 1316844-45-7
ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

Guidance literature:: With palladium diacetate; acetic acid; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol201665c

Reference yield: 76.0%

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 1316844-20-8
ethyl 5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

: 1316844-45-7
ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

Guidance literature:: With palladium diacetate; acetic acid; at 100 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol201665c

Reference yield:

: 3284-51-3
ethyl 5-methyl-1H-pyrrole-2-carboxylate

: 1316844-45-7
ethyl 4-(acetyloxy)-5-methyl-1-(4-methylphenyl)-1H-pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; potassium phosphate; N,N`-dimethylethylenediamine / toluene / 48 h / 110 °C / Inert atmosphere

2: acetic acid / 6 h / 20 °C / Inert atmosphere

3: palladium diacetate; acetic acid / 18 h / 20 °C / Inert atmosphere

With potassium phosphate; copper(l) iodide; palladium diacetate; acetic acid; N,N`-dimethylethylenediamine; In toluene;
DOI:10.1021/ol201665c