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Technology Process of (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

Base Information
  • Chemical Name:(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]
  • CAS No.:166989-45-3
  • Molecular Formula:C24H20B*C48H45O4P3Re
  • Molecular Weight:1284.24
  • Hs Code.:
(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)][B(C<sub>6</sub>H<sub>5</sub>)4]

Synonyms:(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

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Chemical Property of (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]
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Technology Process of (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

There total 7 articles about (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(H)
166989-33-9

(CH3C(CH2P(C6H5)2)3)Re(CO)2(H)

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

propynoic acid ethyl ester
623-47-2

propynoic acid ethyl ester

(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)][B(C<sub>6</sub>H<sub>5</sub>)4]
166989-45-3

(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

Guidance literature:
With HBF4 * OMe2; In ethanol; dichloromethane; N2-atmosphere; stirring (-10°C to room temp.), NaBPh4 soln. (EtOH); evapn. (vac.), extg. (THF), EtOH addn., concg. (N2-stream); elem. anal.;
DOI:10.1021/om9602264

Reference yield: 95.0%

[Re(1,1,1-tris(diphenylphosphanylmethyl)ethane)(CO)2]triflate
222402-52-0

[Re(1,1,1-tris(diphenylphosphanylmethyl)ethane)(CO)2]triflate

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

propynoic acid ethyl ester
623-47-2

propynoic acid ethyl ester

(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)][B(C<sub>6</sub>H<sub>5</sub>)4]
166989-45-3

(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

Guidance literature:
In ethanol; dichloromethane; N2-atmosphere; stirring (-20°C, 30 min), NaBPh4 soln. (EtOH) addn.; elem. anal.;

Reference yield: 95.0%

[(MeC(CH2PPh2)3)Re(CO)2(η(2)-H2)]BF4
166989-35-1

[(MeC(CH2PPh2)3)Re(CO)2(η(2)-H2)]BF4

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

propynoic acid ethyl ester
623-47-2

propynoic acid ethyl ester

(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)Re(CO)2(CC(H)COOC<sub>2</sub>H<sub>5</sub>)][B(C<sub>6</sub>H<sub>5</sub>)4]
166989-45-3

(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)][B(C6H5)4]

Guidance literature:
In ethanol; dichloromethane; N2-atmosphere; stirring (-20°C, 30 min), NaBPh4 soln. (EtOH) addn.; elem. anal.;
upstream raw materials:

(CH3C(CH2P(C6H5)2)3)Re(CO)2(H)

sodium tetraphenyl borate

propynoic acid ethyl ester

[Re(1,1,1-tris(diphenylphosphanylmethyl)ethane)(CO)2]triflate

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