(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

Base Information

Chemical Name:(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate
CAS No.:155085-50-0
Molecular Formula:C₂₃H₃₂O₄
Molecular Weight:372.505
Hs Code.:

Synonyms:(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

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Chemical Property of (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

Chemical Property:

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Technology Process of (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

There total 1 articles about (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5394-63-8
2,2,6-trimethyl-4H-1,3-dioxin-4-one

: 146499-02-7
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydro-1-naphthalenol

: 155085-50-0
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

Guidance literature:: In xylene; at 160 ℃; for 0.5h; preheated bath;
DOI:10.1016/S0040-4020(01)80228-3

Reference yield:

: 155085-50-0
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

: (Z)-3-Amino-but-2-enoic acid (1R,4aS,8S,8aS)-8-(5-methoxy-2-methyl-phenyl)-8-methyl-decahydro-naphthalen-1-yl ester

Guidance literature:: With ammonia; In methanol; for 72h;
DOI:10.1016/S0040-4020(01)80228-3

Reference yield:

: 155085-50-0
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl 3-oxobutanoate

: 155085-51-1
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl (Z)-3-acetamido-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ gas / methanol / 72 h

2: pyridine / tetrahydrofuran / 17 h / Heating

With pyridine; ammonia; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(01)80228-3