Technology Process of dibenzocycloheptene
There total 20 articles about dibenzocycloheptene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
at 400 ℃;
for 1h;
Product distribution;
Mechanism;
"high" pressure;
DOI:10.1021/jo00195a032
- Guidance literature:
-
Multi-step reaction with 8 steps
1: Acidic conditions
2: lithium aluminium tetrahydride / diethyl ether
3: phosphorus tribromide
5: sodium hydroxide
6: sulfuric acid
7: sodium tetrahydroborate / Alkaline conditions
8: Al2O3 supported on acidic zeolites / 300 °C / Flash-vacuum pyrolysis; Inert atmosphere
With
sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; phosphorus tribromide; sodium hydroxide;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: lithium aluminium tetrahydride / diethyl ether
2: phosphorus tribromide
4: sodium hydroxide
5: sulfuric acid
6: sodium tetrahydroborate / Alkaline conditions
7: Al2O3 supported on acidic zeolites / 300 °C / Flash-vacuum pyrolysis; Inert atmosphere
With
sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; phosphorus tribromide; sodium hydroxide;
In
diethyl ether;