4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

Base Information

Chemical Name:4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole
CAS No.:81540-32-1
Molecular Formula:C₃₆H₂₂Cl₄N₄
Molecular Weight:652.409
Hs Code.:

Synonyms:4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

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Chemical Property of 4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

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Technology Process of 4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

There total 4 articles about 4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 623-27-8
terephthalaldehyde,

: 3457-46-3,88372-92-3
4,4'-dichlorobenzil

: 81540-32-1
4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

Guidance literature:: With phosphomolybdic acid; ammonium acetate; In water; acetonitrile; at 80 ℃; for 1h;
DOI:10.1002/jhet.5570450533

Reference yield: 91.0%

: 5216-35-3
1,2-bis(4-chlorophenyl)ethane

: 623-27-8
terephthalaldehyde,

: 81540-32-1
4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

Guidance literature:: With ammonium acetate; In acetic acid; for 2h; Heating;
DOI:10.1007/BF00948252

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 81540-32-1
4,5-di-(4-chlorophenyl)-2-(4-(4,5-di(4-chlorophenyl)-1H-imidazol-2-yl)phenyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: NaCN / dimethylformamide; dimethylsulfoxide

2: 65 percent / ammonium nitrate, Cu(NO₃)2*6H₂O / acetic acid / 2 h / Heating

3: 91 percent / ammonium acetate / acetic acid / 2 h / Heating

With ammonium acetate; ammonium nitrate; sodium cyanide; copper(II) nitrate; In acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1007/BF00948252