N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

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Chemical Name:N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine
CAS No.:1100759-25-8
Molecular Formula:C₄₆H₆₄N₂O₂S₂
Molecular Weight:741.158
Hs Code.:

N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

Synonyms:N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

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Chemical Property of N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

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Technology Process of N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

There total 4 articles about N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 67030-83-5
1,2-bis(4-vinylbenzyl)disulfide

: 61015-94-9
N-(tert-butyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

: 1100759-25-8
N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

Guidance literature:: With sodium tetrahydroborate; 2,2′-((1E,1′E)-(ethane-1,2-diylbis(azanylylidene))bis(methanylylidene))diphenolmanganese(II); In ethanol; toluene;
DOI:10.1016/j.reactfunctpolym.2013.01.009

Reference yield:

: 6987-22-0
amino[(4-ethenylbenzyl)sulfanyl]methanaminium chloride

: 1100759-25-8
N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: sodium hydroxide / 50 °C

3: 2,2′-((1E,1′E)-(ethane-1,2-diylbis(azanylylidene))bis(methanylylidene))diphenolmanganese(II); sodium tetrahydroborate / toluene; ethanol

With sodium tetrahydroborate; 2,2′-((1E,1′E)-(ethane-1,2-diylbis(azanylylidene))bis(methanylylidene))diphenolmanganese(II); sodium hydroxide; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.reactfunctpolym.2013.01.009

Reference yield:

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1100759-25-8
N-tert-butyl-O-{1-[4-(4-{1-[N-tert-butyl-N-(2-methyl-1-phenylpropyl)aminooxy] ethyl}benzyldisulfanylmethyl)phenyl]ethyl}-N-(2-methyl-1-phenylpropyl)hydroxylamine

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 60 °C

2: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

3: sodium hydroxide / 50 °C

4: 2,2′-((1E,1′E)-(ethane-1,2-diylbis(azanylylidene))bis(methanylylidene))diphenolmanganese(II); sodium tetrahydroborate / toluene; ethanol

With sodium tetrahydroborate; 2,2′-((1E,1′E)-(ethane-1,2-diylbis(azanylylidene))bis(methanylylidene))diphenolmanganese(II); sodium hydroxide; In methanol; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.reactfunctpolym.2013.01.009