5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

Base Information

Chemical Name:5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide
CAS No.:1285514-51-3
Molecular Formula:C₂₀H₁₇N₃O₃
Molecular Weight:347.373
Hs Code.:

Synonyms:5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

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Chemical Property of 5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

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Technology Process of 5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

There total 5 articles about 5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285514-50-2
5-formyl-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

: 1285514-51-3
5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In methanol; for 0.25h;

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 1285514-51-3
5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 72 h

2: hydroxylamine hydrochloride; pyridine / methanol / 0.25 h

With pyridine; hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 616-76-2
2-hydroxy-5-formylbenzoic acid

: 1285514-51-3
5-[(E/Z)-(hydroxylmino)methyl]-2-[(phenylmethyl)oxy]-N-3-pyridinylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 24 h

2.1: water; lithium hydroxide / tetrahydrofuran; methanol

2.2: pH 1

3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 72 h

4.1: hydroxylamine hydrochloride; pyridine / methanol / 0.25 h

With pyridine; hydroxylamine hydrochloride; water; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;