(S)-Diethyl 2-phenyl-2-formylglutarate

Base Information

Chemical Name:(S)-Diethyl 2-phenyl-2-formylglutarate
CAS No.:170450-70-1
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

Synonyms:(S)-Diethyl 2-phenyl-2-formylglutarate

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Chemical Property of (S)-Diethyl 2-phenyl-2-formylglutarate

Chemical Property:

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Technology Process of (S)-Diethyl 2-phenyl-2-formylglutarate

There total 7 articles about (S)-Diethyl 2-phenyl-2-formylglutarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 170450-69-8
(S)-Diethyl 2-phenyl-2-(hydroxymethyl)glutarate

: 170450-70-1
(S)-Diethyl 2-phenyl-2-formylglutarate

Guidance literature:: With pyridinium chlorochromate;
DOI:10.1021/jo00122a064

Reference yield:

: 170450-61-0
4,5-Dioxo-3-phenyl-tetrahydro-furan-3-carboxylic acid ethyl ester

: 170450-70-1
(S)-Diethyl 2-phenyl-2-formylglutarate

Guidance literature:: Multi-step reaction with 7 steps

1: 20 percent / D-glucose, bakers' yeast / aq. ethanol / 16 h / 23 °C / bakers' yeastY

2: 76 percent / LiBH₄ / tetrahydrofuran / 5 - 10 °C

3: 73 percent / H₅IO₆ / tetrahydrofuran / 0.17 h

4: 75 percent / CHCl₃ / 1 h / Ambient temperature

5: H₂ / 5percent Pd/C / ethanol

6: HCl / ethanol

7: 73 percent / PCC

With hydrogenchloride; lithium borohydride; D-glucose; bakers' yeast; hydrogen; periodic acid; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jo00122a064

Reference yield:

: 170450-68-7
(S)-Diethyl 4-phenyl-4-<(formyloxy)methyl>glutaconate

: 170450-70-1
(S)-Diethyl 2-phenyl-2-formylglutarate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 5percent Pd/C / ethanol

2: HCl / ethanol

3: 73 percent / PCC

With hydrogenchloride; hydrogen; pyridinium chlorochromate; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00122a064