N-benzylidenebenzylamine hydrochloride

Base Information

Chemical Name:N-benzylidenebenzylamine hydrochloride
CAS No.:87289-85-8
Molecular Formula:C₁₄H₁₄N₂*ClH
Molecular Weight:246.739
Hs Code.:

Synonyms:N-benzylidenebenzylamine hydrochloride

Suppliers and Price of N-benzylidenebenzylamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzylidenebenzylamine hydrochloride

Chemical Property:

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Technology Process of N-benzylidenebenzylamine hydrochloride

There total 2 articles about N-benzylidenebenzylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 20570-96-1
benzylhydrazine dihydrochloride

: 100-52-7
benzaldehyde

: 87289-85-8
N-benzylidenebenzylamine hydrochloride

Guidance literature:: In methanol; for 1h; Heating;

Reference yield: 37.0%

: 6921-34-2
benzylmagnesium chloride

: 87289-85-8
N-benzylidenebenzylamine hydrochloride

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

: 108-88-3,15644-74-3,16713-13-6
toluene

Guidance literature:: benzylmagnesium chloride; With dinitrogen monoxide; In tetrahydrofuran; for 3h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; water; Inert atmosphere;
DOI:10.1021/om500333y

Reference yield:

: 87289-85-8
N-benzylidenebenzylamine hydrochloride

: 87289-84-7
2-benzylhexahydro-1,2,4-triazine-3,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 1) triethylamine; 2) 10percent aq. KOH / 1) ethanol, reflux, 3 days; 2) methanol, reflux, 2 h

2: 1) conc. HCl; 2) conc. H₂SO₄ / 1) water, reflux, 4 h; 2) 6 h, reflux

3: 10 percent / CH₃ONa / methanol / 18 h / Heating

With hydrogenchloride; potassium hydroxide; sulfuric acid; sodium methylate; triethylamine; In methanol;