2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1⁽⁶⁾-cyclohexene-1,2,3,4,5-pentol

Base Information

• Chemical Name: 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1⁽⁶⁾-cyclohexene-1,2,3,4,5-pentol
• CAS No.: 56775-60-1
• Molecular Formula: C₁₉H₂₈O₅
• Molecular Weight: 336.428

Synonyms:2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1⁽⁶⁾-cyclohexene-1,2,3,4,5-pentol

Chemical Property of 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1⁽⁶⁾-cyclohexene-1,2,3,4,5-pentol

Chemical Property:

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Technology Process of 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1⁽⁶⁾-cyclohexene-1,2,3,4,5-pentol

There total 3 articles about 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1⁽⁶⁾-cyclohexene-1,2,3,4,5-pentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Potassium benzoate (582-25-2) + 1L-1,2:3,4-di-O-cyclohexylidene-5-O-methyl-6-O-(trifluoromethylsulfonyl)-chiro-inositol (140195-49-9) → 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1(6)-cyclohexene-1,2,3,4,5-pentol (56775-60-1) + D-3-O-benzoyl-1,2:5,6-di-O-cyclohexylidene-4-O-methyl-myo-inositol (60504-85-0,128442-40-0,131432-85-4,131432-88-7)

Guidance literature:

With 18-crown-6 ether; In N,N-dimethyl-formamide; at 80 ℃; for 4h;

DOI:10.1246/bcsj.65.366

Reference yield: 48.0%

cesium benzoate (17265-04-2) + 1L-1,2:3,4-di-O-cyclohexylidene-5-O-methyl-6-O-(trifluoromethylsulfonyl)-chiro-inositol (140195-49-9) → 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1(6)-cyclohexene-1,2,3,4,5-pentol (56775-60-1) + D-3-O-benzoyl-1,2:5,6-di-O-cyclohexylidene-4-O-methyl-myo-inositol (60504-85-0,128442-40-0,131432-85-4,131432-88-7)

Guidance literature:

With 18-crown-6 ether; In toluene; at 100 ℃; for 10h;

DOI:10.1246/bcsj.65.366

Reference yield: 46.0%

sodium benzoate (532-32-1) + 1L-1,2:3,4-di-O-cyclohexylidene-5-O-methyl-6-O-(trifluoromethylsulfonyl)-chiro-inositol (140195-49-9) → 2D-(2,4,5/3)-2,3:4,5-di-O-cyclohexylidene-1-O-methyl-1(6)-cyclohexene-1,2,3,4,5-pentol (56775-60-1) + D-3-O-benzoyl-1,2:5,6-di-O-cyclohexylidene-4-O-methyl-myo-inositol (60504-85-0,128442-40-0,131432-85-4,131432-88-7)

Guidance literature:

With 18-crown-6 ether; In N,N-dimethyl-formamide; at 45 ℃; for 2h;

DOI:10.1246/bcsj.65.366

upstream raw materials:

sodium benzoate

1L-1,2:3,4-di-O-cyclohexylidene-5-O-methyl-6-O-(trifluoromethylsulfonyl)-chiro-inositol

Potassium benzoate

cesium benzoate

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