3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.0^2,4]non-7-yl ester

Base Information

• Chemical Name: 3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.0^2,4]non-7-yl ester
• CAS No.: 25650-58-2
• Molecular Formula: C₁₇H₁₉NO₅
• Molecular Weight: 317.342

Synonyms:3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.0^2,4]non-7-yl ester

Chemical Property of 3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.0^2,4]non-7-yl ester

Chemical Property:

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Safty Information:

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Technology Process of 3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.0^2,4]non-7-yl ester

There total 5 articles about 3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.0^2,4]non-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-O-Acetylnorscopolamin-hydrochlorid → Norscopolamine (4684-28-0) + (-)-Formylnorscopollamin (25650-58-2)

Guidance literature:

With hydrogenchloride; sodium hydroxide; 1.) H₂O, 2 h, RT; 2.) H₂O, 10 deg C to 15 deg C;

Reference yield:

scopalamine (138-12-5) → nor-(-)-scopolamine (3292-20-4) + 3-Hydroxy-2-phenyl-propionic acid (1R,2R,4S,5S,7S)-9-formyl-3-oxa-9-aza-tricyclo[3.3.1.02,4]non-7-yl ester (25650-58-2)

Guidance literature:

With oxygen; lithium perchlorate; 9,10-Dicyanoanthracene; In acetonitrile; at 20 ℃; Irradiation;

DOI:10.1016/S0040-4039(00)99299-2

Reference yield:

hyoscine hydrobromide (114-49-8) → (-)-Formylnorscopollamin (25650-58-2)

Guidance literature:

With potassium permanganate; potassium carbonate;

DOI:10.1002/jlac.19697290119

upstream raw materials:

hyoscine hydrobromide

(-)-N-Chlorformyl-O-acetylnorscopolamin

9-methyl-3-oxa-9-azatricyclo[3.3.1.0(2,4)]non-7-yl-3'-(acetyloxy)-2'-phenyl propanoate

scopalamine

Downstream raw materials:

(-)-Azoniaspiro-(norscopolamin-8,1'-pyrrolidin)-bromid

Norscopolamine

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