N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide

Base Information

• Chemical Name: N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide
• CAS No.: 861454-89-9
• Molecular Formula: C₅₂H₄₂N₂O₄
• Molecular Weight: 758.916

Synonyms:N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide

Chemical Property of N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide

Chemical Property:

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Technology Process of N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide

There total 4 articles about N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione (324035-44-1) + N-(2,6-diisopropylphenyl)-9-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-perylene-3,4-dicarboximide (695152-67-1) → N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide (861454-89-9)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 80 ℃; for 16h;

DOI:10.1002/chem.200401177

Reference yield:

4-bromo-1,8-naphthalenedicarboxylic anhydride (81-86-7) → N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide (861454-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / ethanol / 12 h / Heating

2: 90 percent / aq. K₂CO₃ / [Pd(PPh₃)4] / toluene / 16 h / 80 °C

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; 2: Suzuki cross-coupling;

DOI:10.1002/chem.200401177

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) → N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide (861454-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / ethanol / 12 h / Heating

2: 90 percent / aq. K₂CO₃ / [Pd(PPh₃)4] / toluene / 16 h / 80 °C

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; 2: Suzuki cross-coupling;

DOI:10.1002/chem.200401177

upstream raw materials:

6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione

N-(2,6-diisopropylphenyl)-9-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-perylene-3,4-dicarboximide

4-bromo-1,8-naphthalenedicarboxylic anhydride

cyclohexylamine

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