6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione

Base Information

• Chemical Name: 6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione
• CAS No.: 324035-44-1
• Molecular Formula: C₁₈H₁₆BrNO₂
• Molecular Weight: 358.235
• Mol file: 324035-44-1.mol

Synonyms:6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione

Chemical Property of 6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione

There total 2 articles about 6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-bromo-1,8-naphthalenedicarboxylic anhydride (81-86-7) + cyclohexylamine (108-91-8,157973-60-9) → 6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione (324035-44-1)

Guidance literature:

In ethanol; for 12h; Heating;

DOI:10.1002/chem.200401177

Reference yield: 82.7%

→ 6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione (324035-44-1)

Guidance literature:

In ethanol; at 80 ℃; for 2h;

Reference yield: 90.0%

6-bromo-2-cyclohexyl-1H-benzo[de]isoquinoline-1,3(2H)-dione (324035-44-1) + N-(2,6-diisopropylphenyl)-9-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-perylene-3,4-dicarboximide (695152-67-1) → N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide (861454-89-9)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 80 ℃; for 16h;

DOI:10.1002/chem.200401177

upstream raw materials:

4-bromo-1,8-naphthalenedicarboxylic anhydride

cyclohexylamine

Downstream raw materials:

N-(2,6-diisopropylphenyl)-9-(4-N-cyclohexylnaphthalene-1,8-dicarboximide)perylene-3,4-dicarboximide

N-(2,6-diisopropylphenyl)-N'-cyclohexylterrylene-3,4:11,12-tetracarboxdiimide

C₄₁H₂₆N₂O₄

C₄₆H₃₄N₂O₄