methyl 4-chloro-2-iodo-6-methylbenzoate

Base Information

Chemical Name:methyl 4-chloro-2-iodo-6-methylbenzoate
CAS No.:1078721-72-8
Molecular Formula:C₉H₈ClIO₂
Molecular Weight:310.519
Hs Code.:

Synonyms:methyl 4-chloro-2-iodo-6-methylbenzoate

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Chemical Property of methyl 4-chloro-2-iodo-6-methylbenzoate

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Technology Process of methyl 4-chloro-2-iodo-6-methylbenzoate

There total 3 articles about methyl 4-chloro-2-iodo-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1048025-62-2
4-chloro-2-iodo-6-methylbenzoic acid

: 74-88-4
methyl iodide

: 1078721-72-8
methyl 4-chloro-2-iodo-6-methylbenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 7499-07-2
4-chloro-2-methylbenzoic acid

: 1078721-72-8
methyl 4-chloro-2-iodo-6-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; [bis(acetoxy)iodo]benzene / palladium diacetate / N,N-dimethyl-formamide / 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With [bis(acetoxy)iodo]benzene; iodine; potassium carbonate; palladium diacetate; In N,N-dimethyl-formamide;

Reference yield:

: 1048025-62-2
4-chloro-2-iodo-6-methylbenzoic acid

: 80-48-8
methyl p-toluene sulfonate

: 1078721-72-8
methyl 4-chloro-2-iodo-6-methylbenzoate

Guidance literature:: 4-chloro-2-iodo-6-methylbenzoic acid; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

methyl p-toluene sulfonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/acs.jmedchem.5b00680