ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate

Base Information

• Chemical Name: ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate
• CAS No.: 750571-43-8
• Molecular Formula: C₂₁H₂₆N₄O₂
• Molecular Weight: 366.463

Synonyms:ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate

Chemical Property of ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate

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Technology Process of ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate

There total 2 articles about ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

6-bromo-N-(2-ethyl-6-methylbenzyl)-2,3-dimethylimidazo[1,2-a]pyrazin-8-amine (750571-41-6) + ethanol (64-17-5) → ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate (750571-43-8)

Guidance literature:

With carbon monoxide; triethylamine; palladium diacetate; triphenylphosphine; at 100 ℃; for 14h; under 7500.75 Torr;

Reference yield: 89.0%

6-bromo-N-(2-ethyl-6-methylbenzyl)-2,3-dimethylimidazo[1,2-a]pyrazin-8-amine (750571-41-6) + ethanol (64-17-5) + carbon monoxide (201230-82-2) → ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate (750571-43-8)

Guidance literature:

With triethylamine; triphenylphosphine; palladium diacetate; at 100 ℃; for 14h; under 7500.75 Torr;

DOI:10.1016/j.bmc.2007.09.009

Reference yield: 95.0%

ethyl 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylate (750571-43-8) → 8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylic acid (750571-45-0)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 80 ℃; for 1h;

DOI:10.1016/j.bmc.2007.09.009

upstream raw materials:

6-bromo-N-(2-ethyl-6-methylbenzyl)-2,3-dimethylimidazo[1,2-a]pyrazin-8-amine

ethanol

carbon monoxide

Downstream raw materials:

8-[(2-ethyl-6-methylbenzyl)amino]-2,3-dimethylimidazo[1,2-a]pyrazine-6-carboxylic acid

C₁₉H₂₄N₄O

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