trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Base Information

Chemical Name:trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate
CAS No.:92078-26-7
Molecular Formula:C₄₂H₄₅N₃O₁₅
Molecular Weight:831.83
Hs Code.:

Synonyms:trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

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Chemical Property of trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

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Technology Process of trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

There total 4 articles about trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 77372-56-6
1,3,5-tris(aminomethyl)benzene

: 75956-64-8
2,3-Dimethoxy-4-(methoxycarbonyl)benzoylchlorid

: 92078-26-7
trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Guidance literature:: With triethylamine; In N,N-dimethyl acetamide; for 4h;
DOI:10.1016/S0040-4020(01)87606-7

Reference yield:

: 60541-32-4
benzene-1,3,5-tricarboxamide

: 92078-26-7
trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium boranate, borontrifluoride etherate, 2.) cc.HCl / 1.) THF, room temperature, 3 d, than reflux, 4 d, 2.) THF, reflux, 4 h

2: 95 percent / triethylamine / N,N-dimethyl-acetamide / 4 h

With hydrogenchloride; sodium metaborate; boron trifluoride diethyl etherate; triethylamine; In N,N-dimethyl acetamide;
DOI:10.1016/S0040-4020(01)87606-7

Reference yield:

: 7168-94-7
dimethyl 2,3-dimethoxyterephthalate

: 92078-26-7
trimethyl-2,2',2,3,3',3-hexamethoxy-4,4',4-<1,3,5-benzenetriyltris(methyleniminocarbonyl)>tris benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / NaOH / methanol; H₂O / Heating

2: 90 percent / thionyl chloride / 0.5 h / Heating

3: 95 percent / triethylamine / N,N-dimethyl-acetamide / 4 h

With sodium hydroxide; thionyl chloride; triethylamine; In methanol; N,N-dimethyl acetamide; water;
DOI:10.1016/S0040-4020(01)87606-7