1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Base Information

Chemical Name:1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene
CAS No.:1026683-76-0
Molecular Formula:C₂₁H₂₁NO₆
Molecular Weight:383.401
Hs Code.:

Synonyms:1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Suppliers and Price of 1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

There total 2 articles about 1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 64-18-6
formic acid

: 88840-49-7
6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalen-1(2H)-one oxime

: 1026683-76-0
1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Guidance literature:: With chloro-trimethyl-silane; acetic anhydride; iron; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;
DOI:10.3987/com-00-s(i)43

Reference yield:

: 88775-66-0
6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalen-1(2H)-one

: 1026683-76-0
1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

2: 87 percent / acetic anhydride; iron powder; TMSCl / dimethylformamide / 0.33 h / 20 °C

With chloro-trimethyl-silane; acetic anhydride; iron; In N,N-dimethyl-formamide; 1: reductiv amidation;
DOI:10.3987/com-00-s(i)43

Reference yield: 100.0%

: 77-78-1
dimethyl sulfate

: 1026683-76-0
1-formamido-6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

: 6,7-methylenedioxy-1-(N-methylformamido)-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalene

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In benzene; at 20 ℃; for 1.5h;
DOI:10.3987/com-00-s(i)43