1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

Base Information

Chemical Name:1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid
CAS No.:106989-09-7
Molecular Formula:C₈H₁₇NO₆*ClH
Molecular Weight:259.687
Hs Code.:

Synonyms:1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

Chemical Property:

Purity/Quality:

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Technology Process of 1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

There total 5 articles about 1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 107079-70-9
1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

: 106989-09-7
1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 24h;
DOI:10.1002/jlac.198719870350

Reference yield:

: 106989-04-2
1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

: 106989-09-7
1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) DMSO/(COCl)2, 2.) ethyldiisopropylamine / 1.) CH₂Cl₂, -78 deg C, 2 h, 2.) room temp., 12 h

2: 23 percent / NH₂OH*HCl / methanol; pyridine / 6 h / Heating

3: 11 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp, 30 min, 2.) 60 deg C, 11 h

4: 99 percent / H₂, 3 N HCl / 10percent Pd/C / methanol / 24 h

With hydrogenchloride; lithium aluminium tetrahydride; oxalyl dichloride; hydroxylamine hydrochloride; hydrogen; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol;
DOI:10.1002/jlac.198719870350

Reference yield:

: 106989-05-3
2L-(2,3,5/4,6)-6-O-benzoyl-2,4,5-tri-O-benzyl-2-C-(benzyloxymethyl)-3-O-methyl-2,3,4,5,6-pentahydroxycyclohexanon

: 106989-09-7
1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 23 percent / NH₂OH*HCl / methanol; pyridine / 6 h / Heating

2: 11 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp, 30 min, 2.) 60 deg C, 11 h

3: 99 percent / H₂, 3 N HCl / 10percent Pd/C / methanol / 24 h

With hydrogenchloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol;
DOI:10.1002/jlac.198719870350