1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Base Information

Chemical Name:1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit
CAS No.:107079-70-9
Molecular Formula:C₃₆H₄₁NO₆
Molecular Weight:583.725
Hs Code.:

Synonyms:1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Suppliers and Price of 1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

There total 4 articles about 1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 107079-35-6
(E)-2L-(2,3,5,6/4)-6-O-benzoyl-2,4,5-tri-O-benzyl-2-C-(benzyloxymethyl)-3-O-methyl-2,3,4,5,6-pentahydroxycyclohexanon-oxim

: 107079-70-9
1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; 1.) room temp, 30 min, 2.) 60 deg C, 11 h;
DOI:10.1002/jlac.198719870350

Reference yield:

: 106989-04-2
1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

: 107079-70-9
1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DMSO/(COCl)2, 2.) ethyldiisopropylamine / 1.) CH₂Cl₂, -78 deg C, 2 h, 2.) room temp., 12 h

2: 23 percent / NH₂OH*HCl / methanol; pyridine / 6 h / Heating

3: 11 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp, 30 min, 2.) 60 deg C, 11 h

With lithium aluminium tetrahydride; oxalyl dichloride; hydroxylamine hydrochloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; pyridine; methanol;
DOI:10.1002/jlac.198719870350

Reference yield:

: 106989-05-3
2L-(2,3,5/4,6)-6-O-benzoyl-2,4,5-tri-O-benzyl-2-C-(benzyloxymethyl)-3-O-methyl-2,3,4,5,6-pentahydroxycyclohexanon

: 107079-70-9
1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / NH₂OH*HCl / methanol; pyridine / 6 h / Heating

2: 11 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp, 30 min, 2.) 60 deg C, 11 h

With lithium aluminium tetrahydride; hydroxylamine hydrochloride; In tetrahydrofuran; pyridine; methanol;
DOI:10.1002/jlac.198719870350