1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

Base Information

Chemical Name:1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit
CAS No.:106989-04-2
Molecular Formula:C₄₃H₄₄O₈
Molecular Weight:688.818
Hs Code.:

Synonyms:1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

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Chemical Property of 1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

Chemical Property:

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Technology Process of 1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

There total 1 articles about 1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-88-4
benzoyl chloride

: 104976-17-2
1L-1,3,4-Tri-O-benzyl-1-C-benzyloxymethyl-2-O-methyl-chiro-inosit

: 106989-04-2
1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

Guidance literature:: With pyridine; In dichloromethane; for 0.25h; Ambient temperature;
DOI:10.1002/jlac.198719870350

Reference yield:

: 106989-04-2
1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

: 106989-09-7
1D-3-amino-3-desoxy-2-C-(hydroxymethyl)-1-O-methyl-epi-inosit-hydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) DMSO/(COCl)2, 2.) ethyldiisopropylamine / 1.) CH₂Cl₂, -78 deg C, 2 h, 2.) room temp., 12 h

2: 23 percent / NH₂OH*HCl / methanol; pyridine / 6 h / Heating

3: 11 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp, 30 min, 2.) 60 deg C, 11 h

4: 99 percent / H₂, 3 N HCl / 10percent Pd/C / methanol / 24 h

With hydrogenchloride; lithium aluminium tetrahydride; oxalyl dichloride; hydroxylamine hydrochloride; hydrogen; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol;
DOI:10.1002/jlac.198719870350

Reference yield:

: 106989-04-2
1L-5-O-benzoyl-1,3,4-tri-O-benzyl-1-C-(benzyloxymethyl)-2-O-methyl-chiro-inosit

: 107079-70-9
1L-3-amino-1,4,6-tri-O-benzyl-4-C-(benzyloxymethyl)-3-desoxy-5-O-methyl-epi-inosit

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DMSO/(COCl)2, 2.) ethyldiisopropylamine / 1.) CH₂Cl₂, -78 deg C, 2 h, 2.) room temp., 12 h

2: 23 percent / NH₂OH*HCl / methanol; pyridine / 6 h / Heating

3: 11 percent / LiAlH₄ / tetrahydrofuran / 1.) room temp, 30 min, 2.) 60 deg C, 11 h

With lithium aluminium tetrahydride; oxalyl dichloride; hydroxylamine hydrochloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; pyridine; methanol;
DOI:10.1002/jlac.198719870350