4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane
CAS No.:1365548-78-2
Molecular Formula:C₁₈H₂₅BO₆
Molecular Weight:348.204
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

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Chemical Property of 4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

Chemical Property:

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Technology Process of 4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

There total 3 articles about 4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 154239-21-1
diethyl 2-Bromoterephthalate

: 73183-34-3
bis(pinacol)diborane

: 1365548-78-2
4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

Guidance literature:: With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; In 1,4-dioxane; at 100 ℃;
DOI:10.1080/00958972.2012.713099

Reference yield:

: 553-94-6
4-bromo-m-xylene

: 1365548-78-2
4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; potassium permanganate / water / Reflux

2: sulfuric acid / water / 12 h / Reflux

3: potassium acetate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 1,4-dioxane / 100 °C

With potassium permanganate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; sulfuric acid; potassium acetate; potassium hydroxide; In 1,4-dioxane; water;
DOI:10.1080/00958972.2012.713099

Reference yield:

: 586-35-6
2-bromo-1,4-benzenedicarboxylic acid

: 1365548-78-2
4,4,5,5-tetramethyl-2-(diethyl 2,5-dicarboxylatephenyl)-1,3-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / water / 12 h / Reflux

2: potassium acetate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 1,4-dioxane / 100 °C

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; sulfuric acid; potassium acetate; In 1,4-dioxane; water;
DOI:10.1080/00958972.2012.713099