N,N-dibenzyl phenylalanin ethyl ester

Base Information

Chemical Name:N,N-dibenzyl phenylalanin ethyl ester
CAS No.:171815-91-1
Molecular Formula:C₂₅H₂₇NO₂
Molecular Weight:373.495
Hs Code.:

Synonyms:N,N-dibenzyl phenylalanin ethyl ester

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Chemical Property of N,N-dibenzyl phenylalanin ethyl ester

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Technology Process of N,N-dibenzyl phenylalanin ethyl ester

There total 3 articles about N,N-dibenzyl phenylalanin ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 3182-93-2
(L)-phenylalanine ethyl ester hydrochloride

: 100-39-0
benzyl bromide

: 171815-91-1
N,N-dibenzyl phenylalanin ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 5h; Reflux;
DOI:10.1021/acs.orglett.8b00864

Reference yield: 29.0%

: 3081-24-1
H-Phe-OEt

: 100-39-0
benzyl bromide

: 171815-91-1
N,N-dibenzyl phenylalanin ethyl ester

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 100 ℃; for 2h; Inert atmosphere; Microwave irradiation;
DOI:10.1039/c4ob00662c

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 171815-91-1
N,N-dibenzyl phenylalanin ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 2 h / 120 °C / Inert atmosphere; Microwave irradiation

2: sodium hydrogencarbonate / tetrahydrofuran / 2 h / 100 °C / Inert atmosphere; Microwave irradiation

With sulfuric acid; sodium hydrogencarbonate; In tetrahydrofuran;
DOI:10.1039/c4ob00662c