3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

Base Information

Chemical Name:3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine
CAS No.:173737-60-5
Molecular Formula:C₁₈H₃₃NO₃Si
Molecular Weight:339.55
Hs Code.:

Synonyms:3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

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Chemical Property of 3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

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Technology Process of 3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

There total 5 articles about 3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65495-21-8
N,N-dimethyl-3,4-dimethoxybenzylamine

: 173737-60-5
3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 4 h, 2.) room temperature, 4 h

2: i-Pr₂NH / CH₂Cl₂ / 1 h

With n-butyllithium; diisopropylamine; In dichloromethane;
DOI:10.1021/jo951611q

Reference yield:

: 6967-45-9
3,4-dimethoxy-N,N-dimethylbenzamide

: 173737-60-5
3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 4 h, 2.) room temperature, 4 h

3: i-Pr₂NH / CH₂Cl₂ / 1 h

With lithium aluminium tetrahydride; n-butyllithium; diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo951611q

Reference yield:

: 93-07-2
Veratric acid

: 173737-60-5
3,4-dimethoxy-N,N-dimethyl-2-(((1,1-dimethylethyl)dimethylsilyl)oxy)methylbenzylamine

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 3 h / Ambient temperature

2: aq. NaOH / CH₂Cl₂ / 12 h

3: 98 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

4: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 4 h, 2.) room temperature, 4 h

5: i-Pr₂NH / CH₂Cl₂ / 1 h

With sodium hydroxide; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo951611q