((t)Bu₂PhSiO)3TaCl₂

Base Information

Chemical Name:((t)Bu₂PhSiO)3TaCl₂
CAS No.:710946-62-6
Molecular Formula:C₄₂H₆₉Cl₂O₃Si₃Ta
Molecular Weight:958.118
Hs Code.:

((t)Bu<sub>2</sub>PhSiO)3TaCl<sub>2</sub>

Synonyms:((t)Bu₂PhSiO)3TaCl₂

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Chemical Property of ((t)Bu₂PhSiO)3TaCl₂

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Technology Process of ((t)Bu₂PhSiO)3TaCl₂

There total 1 articles about ((t)Bu₂PhSiO)3TaCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 710946-61-5
(t)Bu₂PhSiONa

: 7721-01-9
tantalum pentachloride

: 710946-62-6
((t)Bu₂PhSiO)3TaCl₂

Guidance literature:: In benzene; soln. TaCl5 and (t)Bu2PhSiONa in benzene was refluxed for 20 h; solvent was removed in vacuo, residue was triturated with pentane, filtrate was concd. and cooled to -78°C for 4 h; elem. anal.;
DOI:10.1021/ic035407u

Reference yield: 87.0%

: 710946-62-6
((t)Bu₂PhSiO)3TaCl₂

: 1333-74-0
hydrogen

: 710946-63-7
((t)Bu₂PhSiO)3TaH₂

Guidance literature:: With Na/Hg; In diethyl ether; ((t)Bu2PhSiO)3TaCl2 and Na/Hg in Et2O was stirred under 1 atm H2 for 16 h; solvent was removed in vacuo, residue was suspended in pentane and filtered, solvent was evapd.;
DOI:10.1021/ic035407u

Reference yield:

: 503-17-3
dimethylacetylene

: 710946-62-6
((t)Bu₂PhSiO)3TaCl₂

: 710946-85-3
((t)Bu2PhSiO)3Ta(η-C2Me2)

Guidance literature:: With Na/Hg; In diethyl ether; ((t)Bu2PhSiO)3TaCl2, 2-butyne, and Na/Hg in Et2O were stirred at 23°C for 2h; solvent was removed, residue was triturated with pentane, filtrate was evapd.;
DOI:10.1021/ic035407u