8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

Base Information

Chemical Name:8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide
CAS No.:1310693-32-3
Molecular Formula:C₂₃H₃₀ClN₂*I
Molecular Weight:496.862
Hs Code.:

Synonyms:8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

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Chemical Property of 8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

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Technology Process of 8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

There total 5 articles about 8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1310693-54-9
8-chloro-5-(5-cyclohexylpentyl)-5H-pyrido[3,2-b]indole

: 74-88-4
methyl iodide

: 1310693-32-3
8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

Guidance literature:: In toluene; at 110 ℃; for 24h;
DOI:10.1016/j.ejmech.2011.03.021

Reference yield:

: 1268526-01-7
N-(4-chlorophenyl)pyridin-3-amine

: 1310693-32-3
8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium diacetate; trifluoroacetic acid / 6 h / 72 °C

1.2: Cooling with ice

2.1: sodium hydride / 1,2-dimethoxyethane / 12 h / 20 °C

3.1: toluene / 24 h / 110 °C

With palladium diacetate; sodium hydride; trifluoroacetic acid; In 1,2-dimethoxyethane; toluene;
DOI:10.1016/j.ejmech.2011.03.021

Reference yield:

: 54089-03-1
1-bromo-5-cyclohexylpentane

: 1310693-32-3
8-chloro-5-(5-cyclohexylpentyl)-1-methyl-5H-pyrido[3,2-b]indol-1-ium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide / acetone / 12 h / 60 °C

2: sodium hydride / 1,2-dimethoxyethane / 12 h / 20 °C

3: toluene / 24 h / 110 °C

With sodium hydride; sodium iodide; In 1,2-dimethoxyethane; acetone; toluene;
DOI:10.1016/j.ejmech.2011.03.021