N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

Base Information

Chemical Name:N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate
CAS No.:123154-07-4
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:305.374
Hs Code.:

Synonyms:N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

Suppliers and Price of N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

Chemical Property:

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Technology Process of N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

There total 6 articles about N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 123154-06-3
N-acetyl-3-(3-methyl-2-butenyl)oxy-ethyl anthranilate

: 74-88-4
methyl iodide

: 123154-07-4
N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

Guidance literature:: With perhydrodibenzo-18-crown-6; potassium tert-butylate; In diethyl ether; for 0.5h; Heating;
DOI:10.1007/BF00809269

Reference yield:

: 606-13-3
ethyl 2-amino-3-hydroxybenzoate

: 123154-07-4
N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

Guidance literature:: Multi-step reaction with 4 steps

1: 15 percent / pyridine / 16 h / Ambient temperature

2: tBuOK, dicyclohexyl-18 crown 6, CH₃I / diethyl ether / 1.5 h / Heating

3: 99 percent / K₂CO₃ / acetone / 2 h / Heating

4: 89 percent / tBuOK, dicyclohexyl 18 crown 6 / diethyl ether / 0.5 h / Heating

With perhydrodibenzo-18-crown-6; potassium tert-butylate; potassium carbonate; methyl iodide; In pyridine; diethyl ether; acetone;
DOI:10.1007/BF00809269

Reference yield:

: 123154-04-1
N-acetyl-3-hydroxy ethyl anthranilate

: 123154-07-4
N-acetyl-N-methyl-3(3-methyl-2-butenyl)oxy ethyl anthranilate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / K₂CO₃ / acetone / 2 h / Heating

2: 89 percent / tBuOK, dicyclohexyl 18 crown 6 / diethyl ether / 0.5 h / Heating

With perhydrodibenzo-18-crown-6; potassium tert-butylate; potassium carbonate; In diethyl ether; acetone;
DOI:10.1007/BF00809269