(S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid

Base Information

• Chemical Name: (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid
• CAS No.: 92782-33-7
• Molecular Formula: C₁₀H₁₁N₃O₇
• Molecular Weight: 285.213
• Mol file: 92782-33-7.mol

Synonyms:(S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid

Chemical Property of (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid

There total 1 articles about (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

L-valine (72-18-4,25609-85-2,7004-03-7,921-10-8) + 3,5-dinitro-1-(p-nitrophenyl)-4-pyridone (74197-40-3) → 4-nitro-aniline (100-01-6,104810-17-5) + (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid (92782-33-7)

Guidance literature:

In pyridine; water; for 4h; Ambient temperature;

DOI:10.1246/bcsj.57.1961

Reference yield: 87.0%

benzyl bromide (100-39-0) + (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid (92782-33-7) → (S)-2-(3,5-Dinitro-4-oxo-4H-pyridin-1-yl)-3-methyl-butyric acid benzyl ester

Guidance literature:

With N-cyclohexyl-cyclohexanamine;

upstream raw materials:

L-valine

3,5-dinitro-1-(p-nitrophenyl)-4-pyridone