diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:91288-39-0
Molecular Formula:C₂₇H₃₁NO₈S
Molecular Weight:529.611
Hs Code.:

Synonyms:diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

There total 3 articles about diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 51450-09-0
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose

: 776-74-9
Bromodiphenylmethane

: 91288-39-0
diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With potassium carbonate; In water; acetone; for 6h; Ambient temperature;
DOI:10.1016/0008-6215(84)85124-1

Reference yield:

: 51224-18-1
S-thiouronium 2-N-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside hydrochloride

: 91288-39-0
diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / potassium pyrosulfite / H₂O; CHCl₃ / 1.) 85 deg C, 2o min; 2.) rt, 0.5 h.

2: 28 percent / K₂CO₃ / acetone; H₂O / 6 h / Ambient temperature

With potassium disulphite; potassium carbonate; In chloroform; water; acetone;
DOI:10.1016/0008-6215(84)85124-1

Reference yield:

: 91288-31-2
2-acetamido-3,4,6-tri-O-acetyl-1-carbamoyl-2-deoxy-1-thio-β-D-glucopyranose

: 91288-39-0
diphenylmethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / potassium pyrosulfite / H₂O; CHCl₃ / 0.75 h / 85 °C

2: 28 percent / K₂CO₃ / acetone; H₂O / 6 h / Ambient temperature

With potassium disulphite; potassium carbonate; In chloroform; water; acetone;
DOI:10.1016/0008-6215(84)85124-1