3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

Base Information

Chemical Name:3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose
CAS No.:138847-63-9
Molecular Formula:C₁₇H₂₂O₄
Molecular Weight:290.359
Hs Code.:

Synonyms:3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

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Chemical Property of 3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

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Technology Process of 3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

There total 1 articles about 3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 56824-28-3
3,5-anhydro-1,2-O-cyclohexylidene-α-D-xylofuranose

: 100-58-3
phenylmagnesium bromide

: 138847-63-9
3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

Guidance literature:: 3,5-anhydro-1,2-O-cyclohexylidene-α-D-xylofuranose; phenylmagnesium bromide; In tetrahydrofuran; diethyl ether; for 8.5h; Inert atmosphere; Reflux;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Inert atmosphere;
DOI:10.1016/j.ejmech.2010.03.010

Reference yield: 98.0%

: 138847-63-9
3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

: 100-39-0
benzyl bromide

: 1457973-62-4
3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.bmcl.2013.08.069

Reference yield:

: 138847-63-9
3-O-benzyl-1,2-O-cyclohexylidene-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

: 100-39-0
benzyl bromide

: 1457973-64-6
3-O-benzyl-5-deoxy-5-C-phenyl-α-D-xylo-pentofuranose

: 1457973-66-8
3-O-benzyl-5-deoxy-5-C-phenyl-β-D-xylo-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C

2: acetic acid / water / 3 h / Reflux

With sodium hydride; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.08.069