di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

Base Information

Chemical Name:di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane
CAS No.:1599421-99-4
Molecular Formula:C₂₀H₃₄O₃Si
Molecular Weight:350.574
Hs Code.:

Synonyms:di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

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Chemical Property of di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

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Technology Process of di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

There total 3 articles about di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1421460-54-9
4-(di-tert-butylsilanyl)phenol

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 1599421-99-4
di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 48h; Reflux;
DOI:10.1002/cmdc.201300458

Reference yield:

: 106-41-2
4-bromo-phenol

: 1599421-99-4
di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 3 h / 55 °C

1.2: 0.5 h / -65 °C

1.3: 20 °C

2.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 20 °C / Reflux

With sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; mineral oil;
DOI:10.1002/cmdc.201300458

Reference yield:

: 56310-18-0
di-tert-butylchlorosilane

: 1599421-99-4
di-tert-butyl(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)-silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 3 h / 55 °C

1.2: 0.5 h / -65 °C

1.3: 20 °C

2.1: diethylazodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 20 °C / Reflux

With sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; mineral oil;
DOI:10.1002/cmdc.201300458