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5-(1-cyclohexenyl)-pentanophenone

Base Information Edit
  • Chemical Name:5-(1-cyclohexenyl)-pentanophenone
  • CAS No.:389607-99-2
  • Molecular Formula:C17H22O
  • Molecular Weight:242.361
  • Hs Code.:
  • Mol file:389607-99-2.mol
5-(1-cyclohexenyl)-pentanophenone

Synonyms:5-(1-cyclohexenyl)-pentanophenone

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 5-(1-cyclohexenyl)-pentanophenone Edit
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Technology Process of 5-(1-cyclohexenyl)-pentanophenone

There total 12 articles about 5-(1-cyclohexenyl)-pentanophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With Amberlyst 15; In acetone; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(01)00817-1
Guidance literature:
Multi-step reaction with 9 steps
1: 71 percent / pyridine / 24 h / 0 - 5 °C
2: 54 percent / NaI / acetone / 24 h / Heating
3: 94 percent / NaCN / 72 h / 80 °C
4: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C
5: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C
6: 73 percent / pyridine / 48 h / 0 °C
7: 81 percent / NaI / acetone / 24 h / Heating
8: 65 percent / LDA / tetrahydrofuran / 24 h / 0 - 20 °C
9: 69 percent / Amberlyst 15 / acetone / 24 h / 20 °C
With potassium hydroxide; lithium aluminium tetrahydride; Amberlyst 15; sodium cyanide; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; pyridine; diethyl ether; ethanol; water; acetone;
DOI:10.1016/S0040-4020(01)00817-1
Guidance literature:
Multi-step reaction with 10 steps
1: 62 percent / LiAlH4 / diethyl ether / 3 h / 0 - 20 °C
2: 71 percent / pyridine / 24 h / 0 - 5 °C
3: 54 percent / NaI / acetone / 24 h / Heating
4: 94 percent / NaCN / 72 h / 80 °C
5: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C
6: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C
7: 73 percent / pyridine / 48 h / 0 °C
8: 81 percent / NaI / acetone / 24 h / Heating
9: 65 percent / LDA / tetrahydrofuran / 24 h / 0 - 20 °C
10: 69 percent / Amberlyst 15 / acetone / 24 h / 20 °C
With potassium hydroxide; lithium aluminium tetrahydride; Amberlyst 15; sodium cyanide; sodium iodide; lithium diisopropyl amide; In tetrahydrofuran; pyridine; diethyl ether; ethanol; water; acetone;
DOI:10.1016/S0040-4020(01)00817-1
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