Technology Process of C20H34O4Si
There total 4 articles about C20H34O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 36.0 g / (DHQ)2PHAL; K3[Fe(CN)6]; K2CO3 / K2OsO2(OH)4 / 2-methyl-propan-2-ol; H2O / 48 h / 0 °C
2: PPTS / CH2Cl2 / 1.5 h / 20 °C
With
Hydroquinone 1,4-phthalazinediyl diether; pyridinium p-toluenesulfonate; potassium carbonate; potassium hexacyanoferrate(III);
potassium dioxotetrahydroxoosmate(VI);
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo062513f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: DMAP; triethylamine / CH2Cl2 / 0 - 20 °C
2: 36.0 g / (DHQ)2PHAL; K3[Fe(CN)6]; K2CO3 / K2OsO2(OH)4 / 2-methyl-propan-2-ol; H2O / 48 h / 0 °C
3: PPTS / CH2Cl2 / 1.5 h / 20 °C
With
dmap; Hydroquinone 1,4-phthalazinediyl diether; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; potassium hexacyanoferrate(III);
potassium dioxotetrahydroxoosmate(VI);
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo062513f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: DMAP; triethylamine / CH2Cl2 / 0 - 20 °C
2: 36.0 g / (DHQ)2PHAL; K3[Fe(CN)6]; K2CO3 / K2OsO2(OH)4 / 2-methyl-propan-2-ol; H2O / 48 h / 0 °C
3: PPTS / CH2Cl2 / 1.5 h / 20 °C
With
dmap; Hydroquinone 1,4-phthalazinediyl diether; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; potassium hexacyanoferrate(III);
potassium dioxotetrahydroxoosmate(VI);
In
dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo062513f