5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione

Base Information

• Chemical Name: 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione
• CAS No.: 1282531-58-1
• Molecular Formula: C₁₇H₂₃N₃O₄
• Molecular Weight: 333.387

Synonyms:5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione

Chemical Property of 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione

Chemical Property:

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Technology Process of 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione

There total 3 articles about 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]pyrimidine-2,4(1H,3H)-dione (1282531-57-0) + ethyl iodide (75-03-6) → 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione (1282531-58-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 36h;

DOI:10.1515/znb-2010-1212

Reference yield:

2-dimethylaminomethylene-5,5-dimethylcyclohexane-1,3-dione (75039-59-7) → 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione (1282531-58-1)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 8 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1515/znb-2010-1212

Reference yield:

dimedone (126-81-8) → 5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]-1,3-diethylpyrimidine-2,4(1H,3H)-dione (1282531-58-1)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 8 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1515/znb-2010-1212

upstream raw materials:

5-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methylamino]pyrimidine-2,4(1H,3H)-dione

ethyl iodide

2-dimethylaminomethylene-5,5-dimethylcyclohexane-1,3-dione

dimedone

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