tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

Base Information

Chemical Name:tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)
CAS No.:116025-85-5
Molecular Formula:C₄₆H₆₃P₄Rh
Molecular Weight:842.807
Hs Code.:

Synonyms:tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

Suppliers and Price of tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

There total 2 articles about tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 107197-98-8
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

: 19966-81-5
lithium dicyclohexylphosphide

: 116025-85-5
tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

Guidance literature:: In diethyl ether; byproducts: LiCl; N2 atmosphere, slow warming (from ice-cooling to room temp.,), stirring (12 h); solvent removal, digestion (toluene), evapn., extraction (hexane), solvent removal, drying (vacuum); elem. anal.;

Reference yield:

: 116025-84-4
tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

: 116025-85-5
tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

Guidance literature:: Multi-step reaction with 2 steps

1: methyl chloride / toluene

2: diethyl ether

With methyl chloride; In diethyl ether; toluene;