(3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

Base Information

Chemical Name:(3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester
CAS No.:116643-38-0
Molecular Formula:C₂₄H₃₂O₅Si
Molecular Weight:428.601
Hs Code.:

Synonyms:(3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

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Chemical Property of (3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

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Technology Process of (3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

There total 5 articles about (3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 542-05-2
acetonedicarboxylic acid

: 116643-38-0
(3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / HCl gas / 0 °C

2: 91 percent / H₂ / Raney-Ni / propan-1-ol; triethylamine / 25 °C

3: H₂O / pig liver esterase (PLE) / 30 h / 0 °C / pH 7 (0.3 M aqueous KH₂PO₄ and 1N NaOH)

4: imidazol / CH₂Cl₂ / 0 °C

5: H₂O, Na₂CO₃ / 25 °C

With 1H-imidazole; hydrogenchloride; water; hydrogen; sodium carbonate; pig liver esterase; nickel; In propan-1-ol; dichloromethane; triethylamine;
DOI:10.1016/S0040-4039(00)86112-2

Reference yield:

: 116627-53-3
3-Hydroxy-pentanedioic acid dipropyl ester

: 116643-38-0
(3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / pig liver esterase (PLE) / 30 h / 0 °C / pH 7 (0.3 M aqueous KH₂PO₄ and 1N NaOH)

2: imidazol / CH₂Cl₂ / 0 °C

3: H₂O, Na₂CO₃ / 25 °C

With 1H-imidazole; water; sodium carbonate; pig liver esterase; In dichloromethane;
DOI:10.1016/S0040-4039(00)86112-2

Reference yield:

: 53630-64-1
dipropyl 1,3-acetonedicarboxylate

: 116643-38-0
(3S)-3-tert-butyldiphenylsiloxyglutaric acid monopropyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / H₂ / Raney-Ni / propan-1-ol; triethylamine / 25 °C

2: H₂O / pig liver esterase (PLE) / 30 h / 0 °C / pH 7 (0.3 M aqueous KH₂PO₄ and 1N NaOH)

3: imidazol / CH₂Cl₂ / 0 °C

4: H₂O, Na₂CO₃ / 25 °C

With 1H-imidazole; water; hydrogen; sodium carbonate; pig liver esterase; nickel; In propan-1-ol; dichloromethane; triethylamine;
DOI:10.1016/S0040-4039(00)86112-2