N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

Base Information

Chemical Name:N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride
CAS No.:1356862-08-2
Molecular Formula:C₁₈H₂₈N₂O₂*ClH
Molecular Weight:340.893
Hs Code.:

Synonyms:N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

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Chemical Property of N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

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Technology Process of N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

There total 8 articles about N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1356861-75-0
tert-butyl 4-{[3-(4-Methoxyphenyl)pentan-3-yl]carbamoyl}piperidine-1-carboxylate

: 1356862-08-2
N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

Guidance literature:: With hydrogenchloride; In water; ethyl acetate; at 20 ℃; for 16h;
DOI:10.1248/cpb.59.1376

Reference yield:

: 1184761-90-7
3-(4-methoxyphenyl)pentan-3-amine

: 1356862-08-2
N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 20 h / 20 °C / Cooling with ice

2: hydrogenchloride / water; ethyl acetate / 16 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; ethyl acetate; acetonitrile;
DOI:10.1248/cpb.59.1376

Reference yield:

: 1178318-30-3
2-ethyl-2-(4-methoxyphenyl)butanoic acid

: 1356862-08-2
N-[3-(4-methoxyphenyl)pentan-3-yl]piperidine-4-carboxamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: diphenylphosphoranyl azide; triethylamine / toluene / 24 h / 100 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 20 h / 20 °C / Cooling with ice

4: hydrogenchloride / water; ethyl acetate / 16 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; diphenylphosphoranyl azide; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In water; ethyl acetate; toluene; acetonitrile; 1: Curtius rearrangement;
DOI:10.1248/cpb.59.1376